NPTEL : NOC:Advanced NMR Techniques in Solution and Solid-State (Physics)

Co-ordinators : Prof. N. Suryaprakash


Lecture 1 - Introduction to NMR

Lecture 2 - NMR concepts and spin physics - I

Lecture 3 - NMR concepts and spin physics - II

Lecture 4 - Internal interaction parameters and chemical shifts

Lecture 5 - Chemical shifts

Lecture 6 - Scalar couplings

Lecture 7 - Multiplicity patterns of coupled spins and analysis of 1H NMR spectrum

Lecture 8 - Multiplicity pattern and analysis of NMR spectra - II

Lecture 9 - Analysis of NMR spectra and their analysis

Lecture 10 - Heteronuclear NMR

Lecture 11 - Introduction to Fourier series

Lecture 12 - Complex form of Fourier series

Lecture 13 - Fourier theorems

Lecture 14 - Fourier transformation in NMR

Lecture 15 - Pople notation, construction of spin Hamiltonian

Lecture 16 - Quantum mechanical analysis of AX spectra

Lecture 17 - Quantum mechanical analysis of AB spin system

Lecture 18 - Quantum mechanical analysis of coupled spin systems

Lecture 19 - RF pulses and their phases

Lecture 20 - Receiver phase and phase cycling

Lecture 21 - Evolution of chemical shift

Lecture 22 - Evolution of J couplings: polarization transfer

Lecture 23 - selective saturation in homo and heteronuclear spin systems, coupled anddecoupled INEPT

Lecture 24 - INEPT and DEPT

Lecture 25 - Coherence transfer pathway

Lecture 26 - Examples of coherence pathway selection

Lecture 27 - Pulse field gradients - I

Lecture 28 - Pulse field gradients - II

Lecture 29 - Selective excitation, selective inversion

Lecture 30 - Relaxation phenomenon

Lecture 31 - T1 relaxation concepts and measurements

Lecture 32 - Spectral density function and relaxation mechanisms

Lecture 33 - T1 Relaxation mechanisms

Lecture 34 - T1 Relaxation mechanisms and T2 relaxation

Lecture 35 - Measurement of T1 and T2

Lecture 36 - Decoupling and NOE concepts

Lecture 37 - DQ and ZQ relaxation pathways

Lecture 38 - Positive and Negative NOE and spectral density functions

Lecture 39 - NOE and correlation time

Lecture 40 - Product operators

Lecture 41 - Product operator analysis

Lecture 42 - Productor operator analysis of pulse sequences

Lecture 43 - Product operators for two J coupled spins

Lecture 44 - Spin echo sequences

Lecture 45 - Introduction to 2D NMR

Lecture 46 - 2D NMR concepts, 2D experiments

Lecture 47 - 2D COSY experiment

Lecture 48 - 2D COSY and its variants

Lecture 49 - TOCSY Heteronuclear 2D experiments

Lecture 50 - coupled and decoupled HSQC, HMBC, INADEQUATE, 2D Jresolved

Lecture 51 - Introduction to multiple quantum NMR

Lecture 52 - DQ and ZQ of coupled spins

Lecture 53 - MQ and relative signs of couplings

Lecture 54 - MQ and spin system filtering

Lecture 55 - Introduction to solid state NMR

Lecture 56 - CSA and dipolar couplings

Lecture 57 - Magic Angle Spinning

Lecture 58 - WAHUHA and Cross Polarization

Lecture 59 - Cross Polarization

Lecture 60 - CP at high speeds, Side band suppression, TOSS